Technology Process of C37H40N4O5
There total 12 articles about C37H40N4O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dimethylsulfide borane complex / water; tetrahydrofuran / 5.42 h / 0 - 20 °C / Inert atmosphere
2.1: manganese(IV) oxide / chloroform / 2.5 h / Reflux; Inert atmosphere
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
3.2: 4 h / 20 °C / Inert atmosphere
4.1: iron; ammonium chloride / water; ethanol / 1 h / 85 °C / Inert atmosphere
5.1: acetic acid / toluene / Inert atmosphere
With
manganese(IV) oxide; dimethylsulfide borane complex; iron; sodium hydride; ammonium chloride; acetic acid;
In
tetrahydrofuran; ethanol; chloroform; water; toluene;
3.2: |Wittig-Horner Reaction;
DOI:10.1021/jm501532z
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydroxide / dimethyl sulfoxide / 0.67 h / 20 - 75 °C / Inert atmosphere
1.2: 0.17 h / Inert atmosphere
2.1: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dimethyl sulfoxide / 20 °C / Inert atmosphere
3.1: sodium hydroxide / dimethyl sulfoxide / 0.38 h / 60 °C / Inert atmosphere
3.2: Inert atmosphere
4.1: acetic anhydride / 0.67 h / 100 °C / Inert atmosphere
5.1: acetic acid / toluene / Inert atmosphere
With
acetic anhydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; sodium hydroxide;
In
dimethyl sulfoxide; toluene;
DOI:10.1021/jm501532z