dimethylhydrazone of the trimethylsilyl ester of p-methoxybenzoic acid

Base Information

Chemical Name:dimethylhydrazone of the trimethylsilyl ester of p-methoxybenzoic acid
CAS No.:118095-54-8
Molecular Formula:C₁₃H₂₂N₂O₂Si
Molecular Weight:266.415
Hs Code.:

Synonyms:dimethylhydrazone of the trimethylsilyl ester of p-methoxybenzoic acid

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Chemical Property of dimethylhydrazone of the trimethylsilyl ester of p-methoxybenzoic acid

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Technology Process of dimethylhydrazone of the trimethylsilyl ester of p-methoxybenzoic acid

There total 1 articles about dimethylhydrazone of the trimethylsilyl ester of p-methoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 2857-97-8
trimethylsilyl bromide

: 14908-40-8
2,2-dimethylhydrazide of p-methoxybenzoic acid

: 118095-54-8
dimethylhydrazone of the trimethylsilyl ester of p-methoxybenzoic acid

Guidance literature:: With triethylamine; In hexane; at 70 - 80 ℃; for 12h;
DOI:10.1007/BF00957450

Reference yield: 81.0%

: 1719-57-9
Chloro(chloromethyl)dimethylsilane

: 118095-54-8
dimethylhydrazone of the trimethylsilyl ester of p-methoxybenzoic acid

: (Cl-Si)chloro<1-(1,1-dimethyl-2-(4'-methoxybenzoyl)hydrazonium)methyl>dimethylsilane

Guidance literature:: In dichloromethane; for 6h; Ambient temperature;
DOI:10.1016/0022-328X(88)80499-6

Reference yield:

: 118095-54-8
dimethylhydrazone of the trimethylsilyl ester of p-methoxybenzoic acid

: (O-Si)chloro<2-(1,1-dimethyl-2-(4'-methoxybenzoyl)hydrazino)methyl>dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / CH₂Cl₂ / 6 h / Ambient temperature

2: 70 percent / 0.5 h / 170 °C / in an evacuated sealed ampule

In dichloromethane;
DOI:10.1016/0022-328X(88)80499-6