Mn(OC(C₆H₅)CHC(C₆H₅)O)2(C₅H₅N)2⁽¹⁺⁾*ClO₄^(1-)=(Mn(C₁₅H₁₁O₂)2(C₅H₅N)2)ClO₄

Base Information

Chemical Name:Mn(OC(C₆H₅)CHC(C₆H₅)O)2(C₅H₅N)2⁽¹⁺⁾*ClO₄^(1-)=(Mn(C₁₅H₁₁O₂)2(C₅H₅N)2)ClO₄
CAS No.:264216-65-1
Molecular Formula:C₄₀H₃₂MnN₂O₄*ClO₄
Molecular Weight:759.094
Hs Code.:

Mn(OC(C<sub>6</sub>H<sub>5</sub>)CHC(C<sub>6</sub>H<sub>5</sub>)O)2(C<sub>5</sub>H<sub>5</sub>N)2<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=(Mn(C<sub>15</sub>H<sub>11</sub>O<sub>2</sub>)2(C<sub>5</sub>H<sub>5</sub>N)2)ClO<sub>4</sub>

Synonyms:Mn(OC(C₆H₅)CHC(C₆H₅)O)2(C₅H₅N)2⁽¹⁺⁾*ClO₄^(1-)=(Mn(C₁₅H₁₁O₂)2(C₅H₅N)2)ClO₄

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Chemical Property of Mn(OC(C₆H₅)CHC(C₆H₅)O)2(C₅H₅N)2⁽¹⁺⁾*ClO₄^(1-)=(Mn(C₁₅H₁₁O₂)2(C₅H₅N)2)ClO₄

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Technology Process of Mn(OC(C₆H₅)CHC(C₆H₅)O)2(C₅H₅N)2⁽¹⁺⁾*ClO₄^(1-)=(Mn(C₁₅H₁₁O₂)2(C₅H₅N)2)ClO₄

There total 3 articles about Mn(OC(C₆H₅)CHC(C₆H₅)O)2(C₅H₅N)2⁽¹⁺⁾*ClO₄^(1-)=(Mn(C₁₅H₁₁O₂)2(C₅H₅N)2)ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 110-86-1
pyridine

: 35638-41-6
tetra-n-butylammonium permanganate

: manganese(II) perchlorate hexahydrate

: 120-46-7,61346-73-4
1,3-diphenylpropanedione

: 264216-65-1
[Mn(dibenzoylmethanido)₂(pyridine)₂]ClO₄

Guidance literature:: In acetonitrile; soln. of ammonium salt in acetonitrile added dropwise to soln. of Mn perchlorate and pyridine in acetonitrile, addn. of solid dibenzoylmethane, mixt. stirred for a few hours; ppt. filtered off, washed with Et2O, dried under vac.; elem. anal.;
DOI:10.1021/ic049180u

Reference yield: 34.0%

: 110-86-1
pyridine

: 1704-15-0,62961-62-0
3-hydroxy-1,3-diphenyl-2-propen-1-one

: 35638-41-6
tetra-n-butylammonium permanganate

: manganese(II) perchlorate hexahydrate

: 264216-65-1
[Mn(dibenzoylmethanido)₂(pyridine)₂]ClO₄

Guidance literature:: In acetonitrile; for 0.166667h;
DOI:10.1002/ejic.201402964

Reference yield:

: 110-86-1
pyridine

: 35638-41-6
tetra-n-butylammonium permanganate

: manganese(II) perchlorate hexahydrate

: 120-46-7,61346-73-4
1,3-diphenylpropanedione

: 264216-65-1
Mn(OC(C₆H₅)CHC(C₆H₅)O)2(C₅H₅N)2⁽¹⁺⁾*ClO₄^(1-)=(Mn(C₁₅H₁₁O₂)2(C₅H₅N)2)ClO₄

Guidance literature:: In pyridine; ethanol; 2.85 equiv. of Mn(ClO4)2*6H2O and 7.7 equiv. of ligand dissolved in pyridine-EtOH; 1 equiv. of solid NBu4MnO4 added in small portions; several h; filtered; solid washed with EtOH and Et2O; dried in air; recrystd. fromCH2Cl2-Et2O; elem. anal.;
DOI:10.1021/ic991068m