2'-bromo-4',5'-dimethoxybenzoic acid 2-isopropoxy-3-methoxy-5-naphthylamide

Base Information

Chemical Name:2'-bromo-4',5'-dimethoxybenzoic acid 2-isopropoxy-3-methoxy-5-naphthylamide
CAS No.:123719-69-7
Molecular Formula:C₂₃H₂₄BrNO₅
Molecular Weight:474.351
Hs Code.:

Synonyms:2'-bromo-4',5'-dimethoxybenzoic acid 2-isopropoxy-3-methoxy-5-naphthylamide

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Chemical Property of 2'-bromo-4',5'-dimethoxybenzoic acid 2-isopropoxy-3-methoxy-5-naphthylamide

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Technology Process of 2'-bromo-4',5'-dimethoxybenzoic acid 2-isopropoxy-3-methoxy-5-naphthylamide

There total 5 articles about 2'-bromo-4',5'-dimethoxybenzoic acid 2-isopropoxy-3-methoxy-5-naphthylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 52259-69-5
5-amino-2-isopropoxy-3-methoxynaphthalene

: 55171-61-4
2-bromo-4,5-dimethoxybenzoyl chloride

: 123719-69-7
2'-bromo-4',5'-dimethoxybenzoic acid 2-isopropoxy-3-methoxy-5-naphthylamide

Guidance literature:: With N,N-dimethylaminopropane; triethylamine; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 123719-69-7
2'-bromo-4',5'-dimethoxybenzoic acid 2-isopropoxy-3-methoxy-5-naphthylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / KMnO₄ / H₂O; acetone / 1 h / Heating

2: SOCl₂ / CHCl₃ / 1 h / Heating

3: 81 percent / triethylamine, dimethylpropylamine / CH₂Cl₂ / 1 h / 0 °C

With potassium permanganate; thionyl chloride; N,N-dimethylaminopropane; triethylamine; In dichloromethane; chloroform; water; acetone;

Reference yield:

: 6286-46-0
2-bromo-4,5-dimethoxybenzoic acid

: 123719-69-7
2'-bromo-4',5'-dimethoxybenzoic acid 2-isopropoxy-3-methoxy-5-naphthylamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / CHCl₃ / 1 h / Heating

2: 81 percent / triethylamine, dimethylpropylamine / CH₂Cl₂ / 1 h / 0 °C

With thionyl chloride; N,N-dimethylaminopropane; triethylamine; In dichloromethane; chloroform;