2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester

Base Information

• Chemical Name: 2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester
• CAS No.: 243990-73-0
• Molecular Formula: C₁₅H₁₈Cl₂O₂S₂
• Molecular Weight: 365.345
• Mol file: 243990-73-0.mol

Synonyms:2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester

Chemical Property of 2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester

There total 1 articles about 2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

pivaloyl chloride (3282-30-2) + 1-(2,5-Dichlorophenyl)-2,2-bis(methylsulfanyl)ethanone (171897-89-5) → 2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester (243990-73-0)

Guidance literature:

1-(2,5-Dichlorophenyl)-2,2-bis(methylsulfanyl)ethanone; With sodium hydride; In tetrahydrofuran;

pivaloyl chloride; In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1055/s-1999-3529

Reference yield: 92.0%

benzylamine (100-46-9) + 2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester (243990-73-0) → N-benzyl-2,2-dimethylpropanamide (26209-45-0)

Guidance literature:

In tetrahydrofuran; for 4h; Heating;

DOI:10.1055/s-1999-3529

Reference yield: 90.0%

4-Fluorophenol (371-41-5) + 2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester (243990-73-0) → para-fluorophenyl pivalate (183280-13-9)

Guidance literature:

4-Fluorophenol; With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 0.25h;

2,2-dimethyl-propionic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester; In tetrahydrofuran; hexane; for 1h; Heating;

DOI:10.1055/s-1999-3529

upstream raw materials:

pivaloyl chloride

1-(2,5-Dichlorophenyl)-2,2-bis(methylsulfanyl)ethanone

Downstream raw materials:

N-benzyl-2,2-dimethylpropanamide

pivalic acid tert-butyl ester

benzyl pivalate

n-Hexyl pivalate