4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

Base Information

Chemical Name:4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline
CAS No.:1357009-82-5
Molecular Formula:C₃₈H₅₃B₂NO₅
Molecular Weight:625.465
Hs Code.:

Synonyms:4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

Suppliers and Price of 4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

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Technology Process of 4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

There total 8 articles about 4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1104390-10-4
4-bromo-N-(4-bromophenyl)-N-(4-(octyloxy)-phenyl)benzenamine

: 1357009-82-5
4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

Guidance literature:: 4-bromo-N-(4-bromophenyl)-N-(4-(octyloxy)-phenyl)benzenamine; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/c5nj02124c

Reference yield: 62.0%

: 1104390-10-4
4-bromo-N-(4-bromophenyl)-N-(4-(octyloxy)-phenyl)benzenamine

: 73183-34-3
bis(pinacol)diborane

: 1357009-82-5
4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.polymer.2011.12.026

Reference yield:

: 336619-79-5
N,N-bis(4-bromophenyl)-4-hydroxyphenylamine

: 1357009-82-5
4-(octyloxy)-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / butanone / 20 h / Inert atmosphere; Reflux

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 72 h / 80 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; potassium carbonate; In N,N-dimethyl-formamide; butanone;
DOI:10.1016/j.polymer.2011.12.026