(Zn(C₄H₂NC(C₆H₃(C(CH₃)3)2)C₄NH₂CIC₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C))2(Zn(C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C)2)

Base Information

• Chemical Name: (Zn(C₄H₂NC(C₆H₃(C(CH₃)3)2)C₄NH₂CIC₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C))2(Zn(C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C)2)
• CAS No.: 495413-27-9
• Molecular Formula: C₁₄₄H₁₅₀I₂N₁₂Zn₃
• Molecular Weight: 2498.83

Synonyms:(Zn(C₄H₂NC(C₆H₃(C(CH₃)3)2)C₄NH₂CIC₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C))2(Zn(C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C)2)

Chemical Property of (Zn(C₄H₂NC(C₆H₃(C(CH₃)3)2)C₄NH₂CIC₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C))2(Zn(C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C)2)

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Technology Process of (Zn(C₄H₂NC(C₆H₃(C(CH₃)3)2)C₄NH₂CIC₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C))2(Zn(C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C)2)

There total 1 articles about (Zn(C₄H₂NC(C₆H₃(C(CH₃)3)2)C₄NH₂CIC₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C))2(Zn(C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂C)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Zinc(II) 5,15-di(3,5-di-tert-butylphenyl)porphyrin meso-meso trimer (187387-17-3) + iodine (7553-56-2,12190-71-5,8031-47-8) → (Zn(C4H2NC(C6H3(C(CH3)3)2)C4NH2CIC4NH2C(C6H3(C(CH3)3)2)C4NH2C))2(Zn(C4NH2C(C6H3(C(CH3)3)2)C4NH2C)2) (495413-27-9)

Guidance literature:

With AgPF₆; In pyridine; chloroform; acetonitrile; N2 atm.; a soln. of AgPF6 in dry CH3CN was added at 25°C to a soln. of complex and I2 in CHCl3/pyridine 30:1, the mixt. was stirred for 11 min; quenched with H2O, the organic layer was diluted with CHCl3, washed withH2O, satd. aq. NaCl, dried (Na2SO4), evapd. in vac., flash chromy. (sil ica gel; cyclohexane/CH2Cl2 7:3, 1% v/v (C2H5)3N), pptn. from CH2Cl2 upon addn. of CH3OH;

DOI:10.1002/hlca.200590144

Reference yield: 75.0%

(Zn(C4H2NC(C6H3(C(CH3)3)2)C4NH2CIC4NH2C(C6H3(C(CH3)3)2)C4NH2C))2(Zn(C4NH2C(C6H3(C(CH3)3)2)C4NH2C)2) (495413-27-9) + 2-[3-({[(tert-butyl)(dimethyl)silyl]oxy}methyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (495402-49-8) → (Zn(C4H2NC(C6H3(C(CH3)3)2)C4NH2C(C6H4CH2OSi(CH3)2C4H9)C4NH2C(C6H3(C(CH3)3)2)C4NH2C))2(Zn(C4NH2C(C6H3(C(CH3)3)2)C4NH2C)2)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In toluene; mixt. refluxed in C6H5CH3 for 18 h;

DOI:10.1039/b206624f

upstream raw materials:

Zinc(II) 5,15-di(3,5-di-tert-butylphenyl)porphyrin meso-meso trimer

iodine

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