N-methyl-D-glucamine (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Base Information

Chemical Name:N-methyl-D-glucamine (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate
CAS No.:1200445-83-5
Molecular Formula:C₇H₁₇NO₅*C₂₄H₂₂ClNO₄
Molecular Weight:619.112
Hs Code.:

Synonyms:N-methyl-D-glucamine (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

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Chemical Property of N-methyl-D-glucamine (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Chemical Property:

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Technology Process of N-methyl-D-glucamine (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

There total 12 articles about N-methyl-D-glucamine (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-22-3
2-methyl-5-hydroxybenzoic acid

: 1200445-83-5
N-methyl-D-glucamine (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 - 80 °C

2: water; lithium hydroxide / 1,4-dioxane / 20 °C / Inert atmosphere

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: hydrogenchloride; water; acetic acid / 2 h / 90 °C

6: methanol / 20 °C

With hydrogenchloride; oxalyl dichloride; water; potassium carbonate; acetic acid; triethylamine; N,N-dimethyl-formamide; lithium hydroxide; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1034025-63-2
(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

: 6284-40-8,97780-33-1
1-deoxy-1-(methylamino)-D-glucitol

: 1200445-83-5
N-methyl-D-glucamine (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: In methanol; at 20 ℃;

Reference yield:

: 1028543-03-4
ethyl phenylmethyl [3-methyl-4-nitrophenyl]propanedioate

: 1200445-83-5
N-methyl-D-glucamine (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 760.05 Torr

2: triethylamine / dichloromethane / 20 °C

3: hydrogenchloride; water; acetic acid / 2 h / 90 °C

4: methanol / 20 °C

With hydrogenchloride; water; hydrogen; acetic acid; triethylamine; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane;