2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-(3-iodophenyl)ethanol

Base Information

Chemical Name:2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-(3-iodophenyl)ethanol
CAS No.:139140-67-3
Molecular Formula:C₂₄H₃₂IN₃O₂
Molecular Weight:521.441
Hs Code.:

Synonyms:2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-(3-iodophenyl)ethanol

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Chemical Property of 2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-(3-iodophenyl)ethanol

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Technology Process of 2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-(3-iodophenyl)ethanol

There total 2 articles about 2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-(3-iodophenyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: <3-(decyloxy)-6-methylpyridin-2-yl>hydrazone

: 139140-67-3
2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-(3-iodophenyl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NiO₂ / benzene / 72 h / Ambient temperature

2: 1.) LDA / 1.) Et₂O, -40 deg C, 6 h, 2.) Et₂O, from -40 deg C to RT, 14 h

With nickel(IV) oxide; lithium diisopropyl amide; In benzene;
DOI:10.1021/jm00074a013

Reference yield:

: 696-41-3
m-iodobenzaldehyde

: 139140-66-2
4-(decyloxy)-7-methyl<1,2,3>triazolo<1,5-a>pyridine

: 139140-67-3
2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-(3-iodophenyl)ethanol

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) Et₂O, -40 deg C, 6 h, 2.) Et₂O, from -40 deg C to RT, 14 h;
DOI:10.1021/jm00074a013

Reference yield: 72.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 139140-67-3
2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-(3-iodophenyl)ethanol

: 139140-68-4
3-<2-<4-(decyloxy)<1,2,3>triazolo<1,5-a>pyridin-7-yl>-1-hydroxyethyl>benzoic acid methyl ester

Guidance literature:: With palladium diacetate; bis(diphenylphosphino)propane; triethylamine; In dimethyl sulfoxide; at 85 ℃; for 6h;
DOI:10.1021/jm00074a013