mer-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH₂Ph))]PF₆

Base Information

Chemical Name:mer-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH₂Ph))]PF₆
CAS No.:206365-12-0
Molecular Formula:C₅₃H₅₄ClN₂P₂Ru*F₆P
Molecular Weight:1062.46
Hs Code.:

mer-[(CH<sub>3</sub>CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>PPh<sub>2</sub>)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH<sub>2</sub>Ph))]PF<sub>6</sub>

Synonyms:mer-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH₂Ph))]PF₆

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Chemical Property of mer-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH₂Ph))]PF₆

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Technology Process of mer-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH₂Ph))]PF₆

There total 1 articles about mer-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH₂Ph))]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 60969-19-9
thallium(I) hexafluorophosphate

: fac,cis-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl₂(=C(NHPh)CH₂Ph)]

: 536-74-3
phenylacetylene

: 206365-12-0
mer-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH₂Ph))]PF₆

Guidance literature:: With tetrahydrofuran; In tetrahydrofuran; byproducts: TlCl; N2-atmosphere; stirring Ru-complex with 1 equiv. TlPF6 at room temp. for30 min, filtration off of TlCl, addn. of excess PhC2H, stirring for 3 h; crystn. on slow evapn.; elem. anal.;
DOI:10.1016/s0020-1693(97)05877-5

Reference yield: 80.0%

: 206365-12-0
mer-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH₂Ph))]PF₆

: 206365-15-3
[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C_.tplbond.CPh)(C(N(H)Ph)(CH₂Ph))]

Guidance literature:: With tert-butylamine; In tetrahydrofuran; excess amine, 20 min; hexane addn., concn. (under N2); elem. anal.;
DOI:10.1016/s0020-1693(97)05877-5

Reference yield: 80.0%

: 206365-12-0
mer-[(CH₃CH₂CH₂N(CH₂CH₂PPh₂)2)RuCl(C=C(H)Ph)(C(N(H)Ph)(CH₂Ph))]PF₆

: 201230-82-2
carbon monoxide

: 206365-14-2
(CH₃CH₂CH₂N(CH₂CH₂P(C₆H₅)2)2)RuCl(CO)(C(CH₂C₆H₅)NHC₆H₅)⁽¹⁺⁾*PF₆^(1-)=[(C₃₁H₃₅NP₂)RuCl(CO)(C(CH₂C₆H₅)NHC₆H₅)]PF₆

Guidance literature:: In tetrahydrofuran; byproducts: PhC2H; refluxing in CO-atmosphere for 30 min; cooling to room temp., crystn. on hexane addn.; elem. anal.;
DOI:10.1016/s0020-1693(97)05877-5