C₁₉H₂₆FNO₃

Base Information

Chemical Name:C₁₉H₂₆FNO₃
CAS No.:1014703-34-4
Molecular Formula:C₁₉H₂₆FNO₃
Molecular Weight:335.419
Hs Code.:

C<sub>19</sub>H<sub>26</sub>FNO<sub>3</sub>

Synonyms:C₁₉H₂₆FNO₃

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Chemical Property of C₁₉H₂₆FNO₃

Chemical Property:

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Technology Process of C₁₉H₂₆FNO₃

There total 11 articles about C₁₉H₂₆FNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 193537-11-0
tert-butyl 4-(1-cyano-2-ethoxy-2-oxoethylidene)-4-piperidine-1-carboxylate

: 1014703-34-4
C₁₉H₂₆FNO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: copper(l) iodide / tetrahydrofuran / 3 h / 0 °C

2.1: sodium hydroxide / ethanol; water / 15 h / 20 °C

2.2: 0 °C / pH 3

3.1: copper(I) oxide / acetonitrile / 1 - 1.25 h / Heating / reflux

4.1: diisobutylaluminium hydride / dichloromethane / 4 h / -78 - -60 °C

5.1: sodium hypochlorite; sodium carbonate / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 20 °C

6.1: 1,1'-carbonyldiimidazole / dichloromethane / 1 h / 20 °C

6.2: 20 °C

7.1: tetrahydrofuran / 6 h / -78 - 20 °C

With copper(I) oxide; sodium hydroxide; sodium hypochlorite; diisobutylaluminium hydride; sodium carbonate; 1,1'-carbonyldiimidazole; copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 917220-88-3
4-(carboxy-cyano-methyl)-4-(3-fluoro-phenyl)-piperidine-1-carboxylic acid tert-butyl ester

: 1014703-34-4
C₁₉H₂₆FNO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(I) oxide / acetonitrile / 1 - 1.25 h / Heating / reflux

2.1: diisobutylaluminium hydride / dichloromethane / 4 h / -78 - -60 °C

3.1: sodium hypochlorite; sodium carbonate / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 20 °C

4.1: 1,1'-carbonyldiimidazole / dichloromethane / 1 h / 20 °C

4.2: 20 °C

5.1: tetrahydrofuran / 6 h / -78 - 20 °C

With copper(I) oxide; sodium hypochlorite; diisobutylaluminium hydride; sodium carbonate; 1,1'-carbonyldiimidazole; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In tetrahydrofuran; dichloromethane; water; acetonitrile;

Reference yield:

: 878130-37-1
4-cyanomethyl-4-(3-fluoro-phenyl)-piperidine-1-carboxylic acid tert-butyl ester

: 1014703-34-4
C₁₉H₂₆FNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / dichloromethane / 4 h / -78 - -60 °C

2.1: sodium hypochlorite; sodium carbonate / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 20 °C

3.1: 1,1'-carbonyldiimidazole / dichloromethane / 1 h / 20 °C

3.2: 20 °C

4.1: tetrahydrofuran / 6 h / -78 - 20 °C

With sodium hypochlorite; diisobutylaluminium hydride; sodium carbonate; 1,1'-carbonyldiimidazole; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In tetrahydrofuran; dichloromethane; water;