{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-phenyl}-methanol

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Chemical Name:{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-phenyl}-methanol
CAS No.:692205-09-7
Molecular Formula:C₅₆H₆₄Br₂O₈
Molecular Weight:1024.93
Hs Code.:

Synonyms:{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-phenyl}-methanol

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Chemical Property of {3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-phenyl}-methanol

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Technology Process of {3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-phenyl}-methanol

There total 18 articles about {3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-phenyl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 692204-28-7
1-Benzyloxymethyl-3-(3-bromo-propoxy)-5-(3-methyl-benzyloxy)-benzene

: 3-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-5-hydroxymethyl-phenol

: 692205-09-7
{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-phenyl}-methanol

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 12h; Heating;
DOI:10.1021/jo049878p

Reference yield:

: 2050-77-3
Iododecane

: 692205-09-7
{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-phenyl}-methanol

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

2: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

3: 87 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

4: potassium carbonate; 18-crown-6 / tetrahydrofuran / 12 h / Heating

5: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

6: 90 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

With N-Bromosuccinimide; 18-crown-6 ether; dimethylsulfide borane complex; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1021/jo049878p

Reference yield:

: 823-78-9
meta-bromobenzyl bromide

: 692205-09-7
{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-phenyl}-methanol

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

2: water; Dowex-50W-XZ (H⁺ form) / methanol; dioxane / 8 h / Heating

3: potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

4: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

5: 87 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

6: potassium carbonate; 18-crown-6 / tetrahydrofuran / 12 h / Heating

7: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

8: 90 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

With N-Bromosuccinimide; 18-crown-6 ether; dimethylsulfide borane complex; Dowex-50W-XZ (H⁺ form); water; potassium carbonate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; acetone;
DOI:10.1021/jo049878p