2-(benzyloxy)-N,N'-bis(4-{[(benzyloxy)carbonyl]amino}butyl)-N,N'-bis(3-{[(benzyloxy)carbonyl]amino}propyl)-5-(tert-butyl)benzene-1,3-bis[propanamide]

Base Information

Chemical Name:2-(benzyloxy)-N,N'-bis(4-{[(benzyloxy)carbonyl]amino}butyl)-N,N'-bis(3-{[(benzyloxy)carbonyl]amino}propyl)-5-(tert-butyl)benzene-1,3-bis[propanamide]
CAS No.:322638-51-7
Molecular Formula:C₆₉H₈₆N₆O₁₁
Molecular Weight:1175.48
Hs Code.:

Synonyms:2-(benzyloxy)-N,N'-bis(4-{[(benzyloxy)carbonyl]amino}butyl)-N,N'-bis(3-{[(benzyloxy)carbonyl]amino}propyl)-5-(tert-butyl)benzene-1,3-bis[propanamide]

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Chemical Property of 2-(benzyloxy)-N,N'-bis(4-{[(benzyloxy)carbonyl]amino}butyl)-N,N'-bis(3-{[(benzyloxy)carbonyl]amino}propyl)-5-(tert-butyl)benzene-1,3-bis[propanamide]

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Technology Process of 2-(benzyloxy)-N,N'-bis(4-{[(benzyloxy)carbonyl]amino}butyl)-N,N'-bis(3-{[(benzyloxy)carbonyl]amino}propyl)-5-(tert-butyl)benzene-1,3-bis[propanamide]

There total 6 articles about 2-(benzyloxy)-N,N'-bis(4-{[(benzyloxy)carbonyl]amino}butyl)-N,N'-bis(3-{[(benzyloxy)carbonyl]amino}propyl)-5-(tert-butyl)benzene-1,3-bis[propanamide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 89965-56-0
<3-<<4-(carboxyamino)butyl>amino>propyl>carbamic acid, dibenzyl ester

: 322638-50-6
2-(benzyloxy)-5-(tert-butyl)benzene-1,3-bis[propionic acid]

: 322638-51-7
2-(benzyloxy)-N,N'-bis(4-{[(benzyloxy)carbonyl]amino}butyl)-N,N'-bis(3-{[(benzyloxy)carbonyl]amino}propyl)-5-(tert-butyl)benzene-1,3-bis[propanamide]

Guidance literature:: 2-(benzyloxy)-5-(tert-butyl)benzene-1,3-bis[propionic acid]; With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane; at 20 ℃; for 0.5h;

<3-<<4-(carboxyamino)butyl>amino>propyl>carbamic acid, dibenzyl ester; In dichloromethane; at 20 ℃;
DOI:10.1002/1522-2675(20001108)83:11<3021::AID-HLCA3021>3.0.CO;2-E

Reference yield:

: 34911-36-9
4-(tert-butyl)-2,6-di(prop-2-en-1-yl)phenol

: 322638-51-7
2-(benzyloxy)-N,N'-bis(4-{[(benzyloxy)carbonyl]amino}butyl)-N,N'-bis(3-{[(benzyloxy)carbonyl]amino}propyl)-5-(tert-butyl)benzene-1,3-bis[propanamide]

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / dimethylformamide / 1.5 h / 20 °C

1.2: 88 percent / dimethylformamide / 0.5 h / 20 °C

2.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 3.5 h / 65 °C

2.2: 86 percent / 2N NaOH; 30 percent H₂O₂ / 1.5 h / -50 - 20 °C

3.1: 91 percent / 0.54 M H₂CrO₄ / acetone / 3 h / 20 °C

4.1: 1-methyl-2-chloropyridinium iodide; Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

4.2: 93 percent / CH₂Cl₂ / 20 °C

With 2-chloro-1-methyl-pyridinium iodide; chromic acid; sodium hydride; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1002/1522-2675(20001108)83:11<3021::AID-HLCA3021>3.0.CO;2-E

Reference yield:

: 94374-53-5
2-allyl-4-(tert-butyl)phenyl allyl ether

: 322638-51-7
2-(benzyloxy)-N,N'-bis(4-{[(benzyloxy)carbonyl]amino}butyl)-N,N'-bis(3-{[(benzyloxy)carbonyl]amino}propyl)-5-(tert-butyl)benzene-1,3-bis[propanamide]

Guidance literature:: Multi-step reaction with 5 steps

1.1: BCl₃; Et₂O / -10 °C

1.2: methanol / 10 °C

2.1: NaH / dimethylformamide / 1.5 h / 20 °C

2.2: 88 percent / dimethylformamide / 0.5 h / 20 °C

3.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 3.5 h / 65 °C

3.2: 86 percent / 2N NaOH; 30 percent H₂O₂ / 1.5 h / -50 - 20 °C

4.1: 91 percent / 0.54 M H₂CrO₄ / acetone / 3 h / 20 °C

5.1: 1-methyl-2-chloropyridinium iodide; Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

5.2: 93 percent / CH₂Cl₂ / 20 °C

With diethyl ether; 2-chloro-1-methyl-pyridinium iodide; boron trichloride; chromic acid; sodium hydride; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1002/1522-2675(20001108)83:11<3021::AID-HLCA3021>3.0.CO;2-E