o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol

Base Information

• Chemical Name: o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol
• CAS No.: 1145684-33-8
• Molecular Formula: C₁₃H₁₄N₄O
• Molecular Weight: 242.28
• Mol file: 1145684-33-8.mol

Synonyms:o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol

Chemical Property of o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol

There total 2 articles about o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hydrazino-4,6-dimethylpyrimidine (23906-13-0) + salicylaldehyde (90-02-8) → o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol (1145684-33-8)

Guidance literature:

In methanol; Reflux;

DOI:10.1016/j.poly.2012.09.061 DOI:10.1016/j.molstruc.2013.11.004 DOI:10.1016/j.molstruc.2015.02.048

Reference yield:

2-hydrazino-4,6-dimethylpyrimidine (23906-13-0) + 4-(Diethylamino)salicylaldehyde (17754-90-4) → o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol (1145684-33-8)

Guidance literature:

In methanol;

DOI:10.1016/j.jphotochem.2018.03.010

Reference yield: 65.5%

potassium hexafluorophosphate (17084-13-8) + copper(II) perchlorate hexahydrate + o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol (1145684-33-8) + 2,6-Dihydroxybenzoic acid (303-07-1) → C33H35Cu2N8O8*F6P(1-)

Guidance literature:

copper(II) perchlorate hexahydrate; o-[1-(4, 6-dimethylpyrimidine-2-yl)-hydrazonomethyl]-phenol; 2,6-Dihydroxybenzoic acid; In methanol; water; for 1h;

potassium hexafluorophosphate; In methanol; water; for 240h; Cooling;

DOI:10.1016/j.poly.2012.07.075

upstream raw materials:

2-hydrazino-4,6-dimethylpyrimidine

salicylaldehyde

4-(Diethylamino)salicylaldehyde