Technology Process of C18H14BrNO2
There total 4 articles about C18H14BrNO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 100 ℃;
for 0.166667h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; copper diacetate / dichloromethane / 20 °C / Molecular sieve
2: sodium tetrahydroborate / methanol / 0.5 h / 0 - 20 °C
3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.17 h / 100 °C / Microwave irradiation
With
pyridine; sodium tetrahydroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; di-isopropyl azodicarboxylate; copper diacetate; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane;
3: Mitsunobu reaction;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; copper diacetate / dichloromethane / 20 °C / Molecular sieve
2: sodium tetrahydroborate / methanol / 0.5 h / 0 - 20 °C
3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.17 h / 100 °C / Microwave irradiation
With
pyridine; sodium tetrahydroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; di-isopropyl azodicarboxylate; copper diacetate; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane;
3: Mitsunobu reaction;
