[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone

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Chemical Name:[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone
CAS No.:1370344-78-7
Molecular Formula:C₄₉H₄₃F₄N₃O₂
Molecular Weight:781.893
Hs Code.:

Synonyms:[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone

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Chemical Property of [5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone

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Technology Process of [5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone

There total 6 articles about [5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1370344-77-6
11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde

: 134-81-6
benzil

: 1370344-78-7
[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone

Guidance literature:: With ammonium acetate; acetic acid; at 130 ℃; for 3h;

Reference yield:

: 18908-66-2
3-bromomethylheptane

: 1370344-78-7
[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 0 - 20 °C

2.1: trichlorophosphate / 3 h / 0 - 130 °C

3.1: aluminum (III) chloride / dichloromethane / 17 h / 0 - 20 °C

4.1: sodium hydroxide; pyridine / 3 h / 70 °C

5.1: ammonium acetate; acetic acid / 3 h / 130 °C

With pyridine; aluminum (III) chloride; ammonium acetate; sodium hydride; acetic acid; sodium hydroxide; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 239-01-0
11H-benzo[a]carbazole

: 1370344-78-7
[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 0 - 20 °C

2.1: trichlorophosphate / 3 h / 0 - 130 °C

3.1: aluminum (III) chloride / dichloromethane / 17 h / 0 - 20 °C

4.1: sodium hydroxide; pyridine / 3 h / 70 °C

5.1: ammonium acetate; acetic acid / 3 h / 130 °C

With pyridine; aluminum (III) chloride; ammonium acetate; sodium hydride; acetic acid; sodium hydroxide; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide;