N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide

Base Information

Chemical Name:N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide
CAS No.:862134-13-2
Molecular Formula:C₂₆H₂₀F₈N₂O₂
Molecular Weight:544.444
Hs Code.:

Synonyms:N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide

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Chemical Property of N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide

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Technology Process of N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide

There total 7 articles about N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 862132-86-3
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(methylamino)benzamide

: 98-88-4
benzoyl chloride

: 862134-13-2
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide

Guidance literature:: N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(methylamino)benzamide; benzoyl chloride; With pyridine; In tetrahydrofuran; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In tetrahydrofuran; water;

Reference yield:

: 3970-35-2
2-chloro-3-nitrobezoic acid

: 862134-13-2
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 2 h / 80 °C

2.1: pyridine / tetrahydrofuran / 5 h / 20 °C

3.1: potassium fluoride / N,N-dimethyl-formamide / 3 h / 150 °C / Molecular sieve

4.1: hydrogenchloride; tin(ll) chloride / ethanol / 1.5 h / 60 °C

4.2: 20 °C

5.1: sulfuric acid / water / 4 h / 30 - 40 °C

6.1: pyridine / tetrahydrofuran / 3 h / 20 °C

With pyridine; hydrogenchloride; potassium fluoride; thionyl chloride; sulfuric acid; tin(ll) chloride; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 847622-25-7
3-amino-N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluorobenzamide

: 862134-13-2
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / water / 4 h / 30 - 40 °C

2: pyridine / tetrahydrofuran / 3 h / 20 °C

With pyridine; sulfuric acid; In tetrahydrofuran; water;