2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbaldehyde

Base Information

Chemical Name:2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbaldehyde
CAS No.:941693-23-8
Molecular Formula:C₂₀H₂₃NO₄
Molecular Weight:341.407
Hs Code.:

Synonyms:2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbaldehyde

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Chemical Property of 2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbaldehyde

Chemical Property:

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Technology Process of 2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbaldehyde

There total 13 articles about 2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 941693-43-2
2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

: 941693-23-8
2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbaldehyde

Guidance literature:: 2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile; With diisobutylaluminium hydride; In toluene; at -70 ℃; for 0.5h;

With sulfuric acid; In toluene; at 20 ℃; for 3h; Further stages.;
DOI:10.1021/ol070748n

Reference yield:

: 941693-37-4
2-bromo-4,6-dimethyl-3,5-dicarbonitrile

: 941693-23-8
2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; CuI / PdCl₂(PPh₃)2 / diethyl ether / 0.17 h

1.2: 84 percent / diethyl ether / 20 °C

2.1: hydrogen / Pd/C / methanol / 7 h / 2947.82 Torr

3.1: DIBAL-H / toluene / 0.5 h / -70 °C

3.2: 262 mg / aq. H₂SO₄ / toluene / 3 h / 20 °C

With copper(l) iodide; hydrogen; diisobutylaluminium hydride; triethylamine; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; In methanol; diethyl ether; toluene;
DOI:10.1021/ol070748n

Reference yield:

: 4039-83-2
3-(4-methoxybenzyloxy)propyne

: 941693-23-8
2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; CuI / PdCl₂(PPh₃)2 / diethyl ether / 0.17 h

1.2: 84 percent / diethyl ether / 20 °C

2.1: hydrogen / Pd/C / methanol / 7 h / 2947.82 Torr

3.1: DIBAL-H / toluene / 0.5 h / -70 °C

3.2: 262 mg / aq. H₂SO₄ / toluene / 3 h / 20 °C

With copper(l) iodide; hydrogen; diisobutylaluminium hydride; triethylamine; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; In methanol; diethyl ether; toluene;
DOI:10.1021/ol070748n