2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

Base Information

Chemical Name:2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile
CAS No.:941693-43-2
Molecular Formula:C₂₀H₂₁N₃O₂
Molecular Weight:335.406
Hs Code.:

Synonyms:2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

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Chemical Property of 2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

Chemical Property:

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Technology Process of 2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

There total 12 articles about 2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 941693-40-9
2-(3-(4-methoxybenzyloxy)prop-1-ynyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

: 941693-43-2
2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 7h; under 2947.82 Torr;
DOI:10.1021/ol070748n

Reference yield:

: 941693-37-4
2-bromo-4,6-dimethyl-3,5-dicarbonitrile

: 941693-43-2
2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; CuI / PdCl₂(PPh₃)2 / diethyl ether / 0.17 h

1.2: 84 percent / diethyl ether / 20 °C

2.1: hydrogen / Pd/C / methanol / 7 h / 2947.82 Torr

With copper(l) iodide; hydrogen; triethylamine; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1021/ol070748n

Reference yield:

: 4039-83-2
3-(4-methoxybenzyloxy)propyne

: 941693-43-2
2-(3-(4-methoxybenzyloxy)propyl)-4,6-dimethylpyridine-3,5-dicarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; CuI / PdCl₂(PPh₃)2 / diethyl ether / 0.17 h

1.2: 84 percent / diethyl ether / 20 °C

2.1: hydrogen / Pd/C / methanol / 7 h / 2947.82 Torr

With copper(l) iodide; hydrogen; triethylamine; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1021/ol070748n