N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-aminophenoxy)acetamide

Base Information

Chemical Name:N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-aminophenoxy)acetamide
CAS No.:1341199-24-3
Molecular Formula:C₁₅H₁₆ClN₃O₄S
Molecular Weight:369.829
Hs Code.:

Synonyms:N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-aminophenoxy)acetamide

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Chemical Property of N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-aminophenoxy)acetamide

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Technology Process of N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-aminophenoxy)acetamide

There total 6 articles about N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-aminophenoxy)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1341199-23-2
N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide

: 1341199-24-3
N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-aminophenoxy)acetamide

Guidance literature:: With iron; ammonium chloride; In water; acetone; at 80 ℃; for 12h;
DOI:10.1016/j.ejmech.2012.03.032

Reference yield:

: 75263-82-0
C₈H₅Cl₂NO₄

: 1341199-24-3
N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-aminophenoxy)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetone / 2 h / 80 °C

2: ammonium chloride; iron / acetone; water / 12 h / 80 °C

With iron; sodium hydrogencarbonate; ammonium chloride; In water; acetone;
DOI:10.1016/j.ejmech.2012.03.032

Reference yield:

: 21086-49-7
(4-chloro-2-nitro-phenoxy)-acetic acid

: 1341199-24-3
N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-aminophenoxy)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 80 °C

2: sodium hydrogencarbonate / acetone / 2 h / 80 °C

3: ammonium chloride; iron / acetone; water / 12 h / 80 °C

With thionyl chloride; iron; sodium hydrogencarbonate; ammonium chloride; In water; acetone;
DOI:10.1016/j.ejmech.2012.03.032