N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide

Base Information

Chemical Name:N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide
CAS No.:1341199-23-2
Molecular Formula:C₁₅H₁₄ClN₃O₆S
Molecular Weight:399.812
Hs Code.:

Synonyms:N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide

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Chemical Property of N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide

Chemical Property:

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Technology Process of N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide

There total 4 articles about N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75263-82-0
C₈H₅Cl₂NO₄

: 53297-70-4
4-amino-3-methylbenzenesulfonamide

: 1341199-23-2
N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide

Guidance literature:: With sodium hydrogencarbonate; In acetone; at 80 ℃; for 2h;
DOI:10.1016/j.ejmech.2012.03.032

Reference yield:

: 21086-49-7
(4-chloro-2-nitro-phenoxy)-acetic acid

: 1341199-23-2
N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 80 °C

2: sodium hydrogencarbonate / acetone / 2 h / 80 °C

With thionyl chloride; sodium hydrogencarbonate; In acetone;
DOI:10.1016/j.ejmech.2012.03.032

Reference yield:

: 344443-67-0
ethyl 4-chloro-2-nitrophenoxyacetate

: 1341199-23-2
N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide / water; tetrahydrofuran; ethanol / 2 h / 20 °C

2: thionyl chloride / 80 °C

3: sodium hydrogencarbonate / acetone / 2 h / 80 °C

With thionyl chloride; sodium hydrogencarbonate; lithium hydroxide; In tetrahydrofuran; ethanol; water; acetone;
DOI:10.1016/j.ejmech.2012.03.032