1'-benzylspiro hydrochloride

Base Information

• Chemical Name: 1'-benzylspiro hydrochloride
• CAS No.: 75930-61-9
• Molecular Formula: C₂₀H₂₃NO*ClH
• Molecular Weight: 329.87

Synonyms:1'-benzylspiro hydrochloride

Chemical Property of 1'-benzylspiro hydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of 1'-benzylspiro hydrochloride

There total 1 articles about 1'-benzylspiro hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1-benzyl-4-(hydroxymethyl)-4-phenylpiperidine (59083-36-2) → 1'-benzylspiro hydrochloride (75930-61-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 10h; Heating;

DOI:10.1248/cpb.29.402

Reference yield: 32.0%

1'-benzylspiro hydrochloride (75930-61-9) → 1'-benzylspiro-1-one hydrochloride (75930-63-1)

Guidance literature:

With chromium(VI) oxide; In water; acetic acid; at 30 - 35 ℃; for 2.5h;

DOI:10.1248/cpb.29.402

Reference yield:

1'-benzylspiro hydrochloride (75930-61-9) → 1'-benzylspiro-1-one (77607-28-4)

Guidance literature:

With chromium(VI) oxide; acetic acid; In water; for 2.5h;

DOI:10.1021/jm00134a013

upstream raw materials:

formaldehyd

1-benzyl-4-(hydroxymethyl)-4-phenylpiperidine

Downstream raw materials:

1'-benzylspiro-1-one

1'-benzylspiro-1-one hydrochloride

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