N-<(trimethylsilyl)oxy>-N-(phenylmethyl)-α-2-propenylbenzenemethaneamine

Base Information

Chemical Name:N-<(trimethylsilyl)oxy>-N-(phenylmethyl)-α-2-propenylbenzenemethaneamine
CAS No.:133985-92-9
Molecular Formula:C₂₀H₂₇NOSi
Molecular Weight:325.526
Hs Code.:

Synonyms:N-<(trimethylsilyl)oxy>-N-(phenylmethyl)-α-2-propenylbenzenemethaneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(trimethylsilyl)oxy>-N-(phenylmethyl)-α-2-propenylbenzenemethaneamine

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Technology Process of N-<(trimethylsilyl)oxy>-N-(phenylmethyl)-α-2-propenylbenzenemethaneamine

There total 2 articles about N-<(trimethylsilyl)oxy>-N-(phenylmethyl)-α-2-propenylbenzenemethaneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 75-77-4
chloro-trimethyl-silane

: 887239-61-4
N-benzyl-N-(1-phenylbut-3-enyl)hydroxylamine

: 133985-92-9
N-<(trimethylsilyl)oxy>-N-(phenylmethyl)-α-2-propenylbenzenemethaneamine

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/jo00013a032

Reference yield:

: 3376-26-9
N-Benzylidenebenzylamine N-oxide

: 133985-92-9
N-<(trimethylsilyl)oxy>-N-(phenylmethyl)-α-2-propenylbenzenemethaneamine

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / tetrahydrofuran / 0 °C

2: 88 percent / Et₃N / dimethylformamide / Ambient temperature

With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00013a032

Reference yield:

: 133985-92-9
N-<(trimethylsilyl)oxy>-N-(phenylmethyl)-α-2-propenylbenzenemethaneamine

: 133985-98-5,133986-03-5
trans-(2-phenylmethyl)-3-phenyl-5-(iodomethyl)isoxazolidine

: 133985-98-5,133986-03-5
cis-(2-phenylmethyl)-3-phenyl-5-(iodomethyl)isoxazolidine

Guidance literature:: With Iodine monochloride; In dichloromethane; at 0 ℃; for 4h; Yield given. Yields of byproduct given;
DOI:10.1021/jo00013a032