(S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate

Base Information

Chemical Name:(S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate
CAS No.:1320360-29-9
Molecular Formula:C₃₁H₃₀N₂O₆
Molecular Weight:526.589
Hs Code.:

Synonyms:(S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate

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Technology Process of (S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate

There total 3 articles about (S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1320360-23-3
(S)-allyl benzyl piperazine-1,3-dicarboxylate

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1320360-29-9
(S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 13.5h; Inert atmosphere;
DOI:10.1021/ol201912w

Reference yield:

: C₈H₁₄N₂O₂

: 1320360-29-9
(S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / dichloromethane / 13.5 h / 20 °C / Inert atmosphere

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol201912w

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1320360-29-9
(S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / dichloromethane / 13.5 h / 20 °C / Inert atmosphere

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol201912w