(S)-allyl benzyl piperazine-1,3-dicarboxylate

Base Information

Chemical Name:(S)-allyl benzyl piperazine-1,3-dicarboxylate
CAS No.:1320360-23-3
Molecular Formula:C₁₆H₂₀N₂O₄
Molecular Weight:304.346
Hs Code.:

Synonyms:(S)-allyl benzyl piperazine-1,3-dicarboxylate

Suppliers and Price of (S)-allyl benzyl piperazine-1,3-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-allyl benzyl piperazine-1,3-dicarboxylate

Chemical Property:

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Technology Process of (S)-allyl benzyl piperazine-1,3-dicarboxylate

There total 1 articles about (S)-allyl benzyl piperazine-1,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₈H₁₄N₂O₂

: 501-53-1,94274-21-2
benzyl chloroformate

: 1320360-23-3
(S)-allyl benzyl piperazine-1,3-dicarboxylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ol201912w

Reference yield: 98.0%

: 1320360-23-3
(S)-allyl benzyl piperazine-1,3-dicarboxylate

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1320360-29-9
(S)-2-(9H-fluoren-9-yl)methyl 3-allyl 1-benzyl piperazine-1,2,3-tricarboxylate

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 13.5h; Inert atmosphere;
DOI:10.1021/ol201912w

Reference yield:

: 1320360-23-3
(S)-allyl benzyl piperazine-1,3-dicarboxylate

: 138774-72-8
C₂₈H₂₅ClN₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dichloromethane / 13.5 h / 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-methylaniline / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: oxalyl dichloride / dichloromethane / 0 - 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; potassium carbonate; N-methylaniline; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol201912w