1,4-bispentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane

Base Information

• Chemical Name: 1,4-bispentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane
• CAS No.: 156204-98-7
• Molecular Formula: C₃₈H₃₆O₆
• Molecular Weight: 588.7

Synonyms:1,4-bispentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane

Chemical Property of 1,4-bispentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane

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Technology Process of 1,4-bispentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane

There total 1 articles about 1,4-bispentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

cubane-1,4-dicarboxylic acid dimethyl ester (29412-62-2) + 4-methoxyphenyl magnesium bromide (13139-86-1) → 1,4-bispentacyclo<4.2.0.02,5.03,8.04,7>octane (156204-98-7)

Guidance literature:

In tetrahydrofuran; for 1.5h; Heating;

DOI:10.1246/bcsj.67.462

Reference yield: 16.0%

formic acid (64-18-6) + 1,4-bispentacyclo<4.2.0.02,5.03,8.04,7>octane (156204-98-7) → exo-5-formyloxy-8,8-bis(4-methoxyphenyl)-2-tetracyclo<4.3.0.03,9.04,7>nonan-7-ol + 5,9-diformyloxy-6,6,10,10-tetra(4-methoxyphenyl)pentacyclo<5.3.0.02,5.03,9.04,8>decane + 1,4-diformyloxy-5,5,10,10-tetra(4-methoxyphenyl)pentacyclo<5.3.0.02,6.03,9.04,8>decane

Guidance literature:

for 1h; Ambient temperature;

DOI:10.1246/bcsj.67.462

Reference yield: 10.0%

1,4-bispentacyclo<4.2.0.02,5.03,8.04,7>octane (156204-98-7) → 5,5-bis(4-methoxyphenyl)-4-<4-bis(4-methoxyphenyl)methylene-2-cyclobutenyl>-2-cyclopenten-1-one

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; water; for 48h; Ambient temperature;

DOI:10.1246/bcsj.67.462

upstream raw materials:

cubane-1,4-dicarboxylic acid dimethyl ester

4-methoxyphenyl magnesium bromide

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