carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-(3-iodo-propyl)-phenyl ester

Base Information

• Chemical Name: carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-(3-iodo-propyl)-phenyl ester
• CAS No.: 272770-34-0
• Molecular Formula: C₂₂H₃₅IO₃
• Molecular Weight: 474.423

Synonyms:carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-(3-iodo-propyl)-phenyl ester

Chemical Property of carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-(3-iodo-propyl)-phenyl ester

Chemical Property:

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Technology Process of carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-(3-iodo-propyl)-phenyl ester

There total 1 articles about carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-(3-iodo-propyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

di-tert-butyl dicarbonate (24424-99-5) + 4-(3-Iodopropyl)-2, 6-di-tert-butylphenol (224564-43-6) → carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-(3-iodo-propyl)-phenyl ester (272770-34-0)

Guidance literature:

With dmap; In n-heptane;

DOI:10.1016/S0960-894X(02)00698-4

Reference yield: 41.0%

Pentaethylene glycol (4792-15-8) + carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-(3-iodo-propyl)-phenyl ester (272770-34-0) → carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-{3-[2-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-propyl}-phenyl ester (272770-41-9)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 90 ℃;

DOI:10.1016/S0960-894X(02)00698-4

Reference yield: 37.0%

Tetraethylene glycol (112-60-7) + carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-(3-iodo-propyl)-phenyl ester (272770-34-0) → tert-butyl 2,6-di-tert-butyl-4-(15-hydroxy-4,7,10,13-tetraoxapentadecyl)phenyl carbonate (272770-35-1)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 90 ℃;

DOI:10.1016/S0960-894X(02)00698-4

upstream raw materials:

di-tert-butyl dicarbonate

4-(3-Iodopropyl)-2, 6-di-tert-butylphenol

Downstream raw materials:

tert-butyl 2,6-di-tert-butyl-4-(15-hydroxy-4,7,10,13-tetraoxapentadecyl)phenyl carbonate

carbonic acid tert-butyl ester 2,6-di-tert-butyl-4-{3-[2-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-propyl}-phenyl ester

tert-butyl 2,6-di-tert-butyl-4-(15-amino-4,7,10,13-tetraoxapentadecyl)phenyl carbonate

tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate

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