C₂₆H₂₆N₂O₄S

Base Information

Chemical Name:C₂₆H₂₆N₂O₄S
CAS No.:1231976-71-8
Molecular Formula:C₂₆H₂₆N₂O₄S
Molecular Weight:462.569
Hs Code.:

C<sub>26</sub>H<sub>26</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₆H₂₆N₂O₄S

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Chemical Property of C₂₆H₂₆N₂O₄S

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Technology Process of C₂₆H₂₆N₂O₄S

There total 13 articles about C₂₆H₂₆N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1231976-78-5
C₃₂H₃₀N₂O₄S

: 1231976-71-8
C₂₆H₂₆N₂O₄S

Guidance literature:: With Pearlman's catalist; hydrogen; In methanol; water; ethyl acetate; at 23 ℃; for 5h;
DOI:10.1021/ja1030968

Reference yield:

: C₂₅H₂₁NO₆S

: 74-89-5
methylamine

: 1231976-71-8
C₂₆H₂₆N₂O₄S

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; 1,2-dichloro-ethane; at 25 ℃; for 48h; Inert atmosphere;
DOI:10.1002/anie.201006367

Reference yield:

: 1268261-69-3
C₁₇H₁₆F₃NO₇S

: 1231976-71-8
C₂₆H₂₆N₂O₄S

Guidance literature:: Multi-step reaction with 8 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 2.5 h / 70 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 1.5 h / 25 °C

3: pyridine / dichloromethane / 12 h / 25 °C / Inert atmosphere

4: 20% palladium(II) hydroxide on carbon; hydrogen / ethyl acetate / 1.5 h / 25 °C

5: water; acetic acid / 20 h / 25 °C / Inert atmosphere

6: bis-[(trifluoroacetoxy)iodo]benzene / dichloromethane / 0.5 h / -5 - 0 °C / Inert atmosphere

7: lead(IV) tetraacetate; sodium hydrogencarbonate / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

8: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran; 1,2-dichloro-ethane / 48 h / 25 °C / Inert atmosphere

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 20% palladium(II) hydroxide on carbon; palladium 10% on activated carbon; water; hydrogen; lead(IV) tetraacetate; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; sodium carbonate; acetic acid; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; 1: Suzuki-Miyaura reaction;
DOI:10.1002/anie.201006367