C₂₆H₃₅F₂N₃O₃

Base Information

Chemical Name:C₂₆H₃₅F₂N₃O₃
CAS No.:960391-50-8
Molecular Formula:C₂₆H₃₅F₂N₃O₃
Molecular Weight:475.579
Hs Code.:

C<sub>26</sub>H<sub>35</sub>F<sub>2</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₂₆H₃₅F₂N₃O₃

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Chemical Property of C₂₆H₃₅F₂N₃O₃

Chemical Property:

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Technology Process of C₂₆H₃₅F₂N₃O₃

There total 10 articles about C₂₆H₃₅F₂N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960391-38-2
methyl [1-({2-tert-butyl-1-[(4,4-difluorocyclohexyl)methyl]-1H-benzimidazol-5-yl}carbonyl)piperidin-4-yl]acetate

: 960391-50-8
C₂₆H₃₅F₂N₃O₃

Guidance literature:: methyl [1-({2-tert-butyl-1-[(4,4-difluorocyclohexyl)methyl]-1H-benzimidazol-5-yl}carbonyl)piperidin-4-yl]acetate; With lithium hydroxide; water; In 1,4-dioxane; at 75 ℃; for 2h;

With potassium hydrogensulfate; In water; pH=5 - 6;

Reference yield:

: 809273-65-2
(4,4-difluorocyclohexane)methylamine hydrochloride

: 960391-50-8
C₂₆H₃₅F₂N₃O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 75 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 48 h / 20 °C / 2585.81 Torr

3.1: dmap / dichloromethane / 4 h / 20 °C

4.1: acetic acid / 3 h / 150 °C / Microwave irradiation

5.1: lithium hydroxide; water / 1,4-dioxane / 3 h / 75 °C

5.2: pH 5 - 6

6.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

7.1: lithium hydroxide; water / 1,4-dioxane / 2 h / 75 °C

7.2: pH 5 - 6

With dmap; lithium hydroxide; water; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; HATU; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 809273-66-3
methyl {[(4,4-difluorocyclohexyl)methanol]amino}-3-nitrobenzoate

: 960391-50-8
C₂₆H₃₅F₂N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 48 h / 20 °C / 2585.81 Torr

2.1: dmap / dichloromethane / 4 h / 20 °C

3.1: acetic acid / 3 h / 150 °C / Microwave irradiation

4.1: lithium hydroxide; water / 1,4-dioxane / 3 h / 75 °C

4.2: pH 5 - 6

5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

6.1: lithium hydroxide; water / 1,4-dioxane / 2 h / 75 °C

6.2: pH 5 - 6

With dmap; lithium hydroxide; water; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; HATU; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;