C₃₀H₃₉N₃O₇S

Base Information

Chemical Name:C₃₀H₃₉N₃O₇S
CAS No.:1366595-52-9
Molecular Formula:C₃₀H₃₉N₃O₇S
Molecular Weight:585.722
Hs Code.:

C<sub>30</sub>H<sub>39</sub>N<sub>3</sub>O<sub>7</sub>S

Synonyms:C₃₀H₃₉N₃O₇S

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Chemical Property of C₃₀H₃₉N₃O₇S

Chemical Property:

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Technology Process of C₃₀H₃₉N₃O₇S

There total 5 articles about C₃₀H₃₉N₃O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1366595-51-8
C₂₉H₃₇N₃O₅

: 124-63-0
methanesulfonyl chloride

: 1366595-52-9
C₃₀H₃₉N₃O₇S

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.01.098

Reference yield:

: 851544-48-4
(3aS,5R,7aS,9aS)-3-benzyl-4-oxo-decahydro-2-oxa-3,4a-diazacyclopenta[f]azulene-5-carboxylic acid tert-butyl ester

: 1366595-52-9
C₃₀H₃₉N₃O₇S

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylsilane; trifluoroacetic acid / dichloromethane / 4 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / Inert atmosphere

2.2: 18 h / 20 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / ethanol; water / 3 h / 85 °C / 7500.75 Torr

4.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With triethylsilane; palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2012.01.098

Reference yield:

: 1366595-48-3
C₁₈H₂₂N₂O₄

: 1366595-52-9
C₃₀H₃₉N₃O₇S

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: palladium on activated charcoal; hydrogen / ethanol; water / 3 h / 85 °C / 7500.75 Torr

3.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2012.01.098