7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose

Base Information

Chemical Name:7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose
CAS No.:142010-61-5
Molecular Formula:C₂₇H₃₈O₇Si
Molecular Weight:502.68
Hs Code.:

Synonyms:7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose

Suppliers and Price of 7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose

There total 3 articles about 7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 142010-61-5
7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) oxolane, 0 deg C, 30 min, 2) r.t., 12 h

2: 1.) butyllithium / 1.) oxolane, 0 deg C, 1.5 h, 2.) 1 h

With n-butyllithium; sodium hydride;
DOI:10.1016/S0008-6215(00)90560-3

Reference yield:

: 124582-54-3,124582-55-4
6-deoxy-7-C-(2-furyl)-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galacto-heptopyranose

: 142010-61-5
7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) oxolane, 0 deg C, 30 min, 2) r.t., 12 h

2: 1.) butyllithium / 1.) oxolane, 0 deg C, 1.5 h, 2.) 1 h

With n-butyllithium; sodium hydride;
DOI:10.1016/S0008-6215(00)90560-3

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 142010-60-4
(3aR,5R,5aS,8aS,8bR)-5-((R)-2-Benzyloxy-2-furan-2-yl-ethyl)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran

: 142010-61-5
7-O-benzyl-6-deoxy-1,2:3,4-di-O-isopropylidene-7-C-(5-trimethylsilyl-2-furyl)-L-glycero-α-D-galacto-heptopyranose

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) oxolane, 0 deg C, 1.5 h, 2.) 1 h;
DOI:10.1016/S0008-6215(00)90560-3