5-N-carbobenzoxylamino-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosidonic acid

Base Information

Chemical Name:5-N-carbobenzoxylamino-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosidonic acid
CAS No.:145552-07-4
Molecular Formula:C₁₇H₂₃NO₁₀
Molecular Weight:401.37
Hs Code.:

Synonyms:5-N-carbobenzoxylamino-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosidonic acid

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Chemical Property of 5-N-carbobenzoxylamino-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosidonic acid

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Technology Process of 5-N-carbobenzoxylamino-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosidonic acid

There total 4 articles about 5-N-carbobenzoxylamino-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosidonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3006-58-4,7474-40-0,13030-01-8,42890-10-8,42973-23-9,77059-32-6,121785-09-9
2-<(benzyloxycarbonyl)amino>-2-deoxy-D-mannopyranose

: 113-24-6
sodium pyruvate

: 145552-07-4
5-N-carbobenzoxylamino-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosidonic acid

Guidance literature:: With Neu₅Ac aldolase; at 37 ℃; for 24h; Neu₅Ac aldolase, tris-buffer, pH 7.6;
DOI:10.1016/S0040-4020(01)80502-0

Reference yield:

: 4710-95-6,6730-09-2,14131-59-0,14131-62-5,14131-63-6,14131-65-8,14131-67-0,14257-79-5,19124-46-0,20706-90-5,91673-92-6
D-mannosamine hydrochloride

: 145552-07-4
5-N-carbobenzoxylamino-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosidonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / aq. NaHCO₃ / 4 h / Ambient temperature

2: 75 percent / Neu₅Ac aldolase / 24 h / 37 °C / Neu₅Ac aldolase, tris-buffer, pH 7.6

With Neu₅Ac aldolase; sodium hydrogencarbonate;
DOI:10.1016/S0040-4020(01)80502-0

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 145552-07-4
5-N-carbobenzoxylamino-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosidonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / aq. NaHCO₃ / 4 h / Ambient temperature

2: 75 percent / Neu₅Ac aldolase / 24 h / 37 °C / Neu₅Ac aldolase, tris-buffer, pH 7.6

With Neu₅Ac aldolase; sodium hydrogencarbonate;
DOI:10.1016/S0040-4020(01)80502-0