N,N-dibutylthioformamide

Base Information

• Chemical Name: N,N-dibutylthioformamide
• CAS No.: 13749-55-8
• Molecular Formula: C9H19NS
• Molecular Weight: 173.323
• Mol file: 13749-55-8.mol

Synonyms:

Chemical Property of N,N-dibutylthioformamide

Chemical Property:

• Vapor Pressure: 0.000724mmHg at 25°C
• Boiling Point: 307.5°C at 760 mmHg
• Flash Point: 139.7°C
• Density: 0.914g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-dibutylthioformamide

There total 7 articles about N,N-dibutylthioformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.8%

N,N-dibutylformamide (761-65-9) → N,N-di-n-butylthioformamide (13749-55-8)

Guidance literature:

With tetraphosphorus decasulfide;

Reference yield: 46.0%

dibutylamine (111-92-2) + N-phenyl-1,2,3,4,5,7-pentathioazocane (419532-33-5) → N,N-di-n-butylthioformamide (13749-55-8)

Guidance literature:

In benzene; for 7h; Reflux;

DOI:10.1080/10426501003773407

Reference yield: 14.0%

carbon monosulfide (2944-05-0,767590-23-8) + dibutylamine (111-92-2) → N,N-di-n-butylthioformamide (13749-55-8)

Guidance literature:

In toluene; at -78 ℃; under 0.05 Torr;

DOI:10.1021/jo00382a038

upstream raw materials:

hydrogen cyanide

dibutylamine

ethyl thioformate

N,N-dibutylformamide

Downstream raw materials:

2,2-dicyclohexyl-2-hydroxy-N,N-dibutylthioacetamide

2-hydroxy-2-phenyl-N,N-dibutylthioacetamide

N,N-dibutyl-2,2-diphenyl-2-hydroxy-thioacetamide