O-cyclohexyl phenylphenylphosphinate

Base Information

Chemical Name:O-cyclohexyl phenylphenylphosphinate
CAS No.:1706-93-0
Molecular Formula:C₁₈H₂₁O₂P
Molecular Weight:300.337
Hs Code.:

Synonyms:O-cyclohexyl phenylphenylphosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-cyclohexyl phenylphenylphosphinate

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Technology Process of O-cyclohexyl phenylphenylphosphinate

There total 13 articles about O-cyclohexyl phenylphenylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1707-03-5
diphenyl-phosphinic acid

: 108-93-0
cyclohexanol

: 1706-93-0
O-cyclohexyl phenylphenylphosphinate

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 12h; Schlenk technique; Inert atmosphere;

Reference yield: 84.0%

: 4559-70-0
Diphenylphosphine oxide

: 108-93-0
cyclohexanol

: 1706-93-0
O-cyclohexyl phenylphenylphosphinate

Guidance literature:: With 1,10-Phenanthroline; iron(II) acetylacetonate; potassium carbonate; In toluene; at 130 ℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1039/c6dt02236g

Reference yield: 77.0%

: cyclohexyl phenyl-H-phosphinate

: 108-90-7
chlorobenzene

: 1706-93-0
O-cyclohexyl phenylphenylphosphinate

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; at 115 ℃; for 24h; Reagent/catalyst; Inert atmosphere;
DOI:10.1002/adsc.201300069