Technology Process of C18H24O5
There total 6 articles about C18H24O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
2.1: dimethylsulfide borane complex / tetrahydrofuran / -78 °C / Inert atmosphere
3.1: pyridinium chlorochromate / dichloromethane / 5 h / 20 °C
4.1: ammonium cerium (IV) nitrate / acetonitrile; water / 0 °C
5.1: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C
5.2: 2 h / 20 °C
With
dmap; ammonium cerium (IV) nitrate; dimethylsulfide borane complex; triethylamine; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pyridinium chlorochromate / dichloromethane / 24 h / 20 °C
2.1: tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
3.1: dimethylsulfide borane complex / tetrahydrofuran / -78 °C / Inert atmosphere
4.1: pyridinium chlorochromate / dichloromethane / 5 h / 20 °C
5.1: ammonium cerium (IV) nitrate / acetonitrile; water / 0 °C
6.1: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C
6.2: 2 h / 20 °C
With
dmap; ammonium cerium (IV) nitrate; dimethylsulfide borane complex; triethylamine; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;