3-cyclohexylsalicyl alcohol

Base Information

Chemical Name:3-cyclohexylsalicyl alcohol
CAS No.:73779-18-7
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

Synonyms:3-cyclohexylsalicyl alcohol

Suppliers and Price of 3-cyclohexylsalicyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-cyclohexylsalicyl alcohol

Chemical Property:

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Technology Process of 3-cyclohexylsalicyl alcohol

There total 6 articles about 3-cyclohexylsalicyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 119-42-6
2-cyclohexylphenol

: 73779-18-7
3-cyclohexylsalicyl alcohol

Guidance literature:: In 1,2-dimethoxyethane; xylene; at 135 ℃; for 12h;
DOI:10.1055/s-1980-28942

Reference yield:

: 876911-15-8
3-bromosalicyl alcohol isopropylidene acetal

: 931-50-0
cyclohexylmagnesium bromide

: 73779-18-7
3-cyclohexylsalicyl alcohol

Guidance literature:: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 16h;
DOI:10.1081/NCN-200061791

Reference yield:

: 28165-46-0
3-bromo-2-hydroxybenzyl alcohol

: 73779-18-7
3-cyclohexylsalicyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / p-TsOH; Na₂SO₄ / acetone / 72 h / 40 °C

2: Pd(dppf)Cl₂ / diethyl ether; tetrahydrofuran / 16 h / 20 °C

With toluene-4-sulfonic acid; sodium sulfate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; diethyl ether; acetone; 2: Grignard cross-coupling;
DOI:10.1081/NCN-200061791