2-(N-2-methylbenzyl-N-2,4,6-trimethylbenzyl)amino-1-phenylpropylpropionate

Base Information

Chemical Name:2-(N-2-methylbenzyl-N-2,4,6-trimethylbenzyl)amino-1-phenylpropylpropionate
CAS No.:331956-11-7
Molecular Formula:C₃₀H₃₇NO₂
Molecular Weight:443.629
Hs Code.:

Synonyms:2-(N-2-methylbenzyl-N-2,4,6-trimethylbenzyl)amino-1-phenylpropylpropionate

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Chemical Property of 2-(N-2-methylbenzyl-N-2,4,6-trimethylbenzyl)amino-1-phenylpropylpropionate

Chemical Property:

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Technology Process of 2-(N-2-methylbenzyl-N-2,4,6-trimethylbenzyl)amino-1-phenylpropylpropionate

There total 4 articles about 2-(N-2-methylbenzyl-N-2,4,6-trimethylbenzyl)amino-1-phenylpropylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 79-03-8
propionyl chloride

: 331956-09-3
(1R,2S)-2-[(2-methylbenzyl)(2,4,6-trimethylbenzylamino)]-1-phenylpropan-1-ol

: 331956-11-7
2-(N-2-methylbenzyl-N-2,4,6-trimethylbenzyl)amino-1-phenylpropylpropionate

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 5h;
DOI:10.1021/jo001293h

Reference yield:

: 487-68-3
mesytaldehyde

: 331956-11-7
2-(N-2-methylbenzyl-N-2,4,6-trimethylbenzyl)amino-1-phenylpropylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1.1: MgSO₄ / toluene / 6 h / 80 °C

1.2: 65 percent / AcOH; NaCNBH₃ / methanol / 3 h / 20 °C

2.1: 95 percent / toluene; acetonitrile / 1 h / 90 °C

3.1: 93 percent / DMAP / CH₂Cl₂ / 5 h / 0 - 20 °C

With dmap; magnesium sulfate; In dichloromethane; toluene; acetonitrile;
DOI:10.1021/jo001293h

Reference yield:

: 492-41-1,58550-13-3,757124-50-8
(1R,2S)-norephedrine

: 331956-11-7
2-(N-2-methylbenzyl-N-2,4,6-trimethylbenzyl)amino-1-phenylpropylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1.1: MgSO₄ / toluene / 6 h / 80 °C

1.2: 65 percent / AcOH; NaCNBH₃ / methanol / 3 h / 20 °C

2.1: 95 percent / toluene; acetonitrile / 1 h / 90 °C

3.1: 93 percent / DMAP / CH₂Cl₂ / 5 h / 0 - 20 °C

With dmap; magnesium sulfate; In dichloromethane; toluene; acetonitrile;
DOI:10.1021/jo001293h