3-oxobutyric acid 3-phenylprop-2-ynyl ester

Base Information

Chemical Name:3-oxobutyric acid 3-phenylprop-2-ynyl ester
CAS No.:57727-97-6
Molecular Formula:C₁₃H₁₂O₃
Molecular Weight:216.236
Hs Code.:

Synonyms:3-oxobutyric acid 3-phenylprop-2-ynyl ester

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Chemical Property of 3-oxobutyric acid 3-phenylprop-2-ynyl ester

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Technology Process of 3-oxobutyric acid 3-phenylprop-2-ynyl ester

There total 2 articles about 3-oxobutyric acid 3-phenylprop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: 5394-63-8
2,2,6-trimethyl-4H-1,3-dioxin-4-one

: 57727-97-6
3-oxobutyric acid 3-phenylprop-2-ynyl ester

Guidance literature:: In xylene; at 140 ℃; for 2h;
DOI:10.1055/s-1997-740

Reference yield:

: 674-82-8,2130-41-8
4-methyleneoxetan-2-one

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: 57727-97-6
3-oxobutyric acid 3-phenylprop-2-ynyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 25 ℃; for 12h;
DOI:10.1016/S0040-4039(00)97184-3

Reference yield: 91.0%

: 57727-97-6
3-oxobutyric acid 3-phenylprop-2-ynyl ester

: 100-39-0
benzyl bromide

: 187337-12-8
2-benzyl-3-oxobutyric acid 3-phenylprop-2-ynyl

Guidance literature:: 3-oxobutyric acid 3-phenylprop-2-ynyl ester; With sodium hydride; In tetrahydrofuran; at 25 ℃; for 0.5h;

benzyl bromide; In tetrahydrofuran; at 60 ℃; for 4h; Further stages.;
DOI:10.1021/jo991938h