3-chlorocyclohexanol

Base Information

• Chemical Name: 3-chlorocyclohexanol
• CAS No.: 31968-46-4
• Molecular Formula: C₆H₁₁ClO
• Molecular Weight: 134.606
• Mol file: 31968-46-4.mol

Synonyms:3-chlorocyclohexanol

Chemical Property of 3-chlorocyclohexanol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3-chlorocyclohexanol

There total 1 articles about 3-chlorocyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexenone (930-68-7) → 3-chlorocyclohexanol (31968-46-4)

Guidance literature:

With hydrogenchloride; lithium aluminium tetrahydride; Multistep reaction; 1.) Et₂O;

DOI:10.1021/jo980119e

Reference yield:

3-chlorocyclohexanol (31968-46-4) → 3-chlorocyclohexanone (21299-27-4)

Guidance literature:

With 2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl; oxygen; vanadium(V) oxychloride; In acetonitrile; at 80 ℃; for 15h; under 6000.6 Torr;

Reference yield:

3-chlorocyclohexanol (31968-46-4) + methyl iodide (74-88-4) → cis-3-chloro-1-methoxycyclohexane + trans-3-chloro-1-methoxycyclohexane

Guidance literature:

3-chlorocyclohexanol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h;

methyl iodide; In tetrahydrofuran; for 1.5h; Title compound not separated from byproducts; Heating;

DOI:10.1016/j.saa.2004.12.001

upstream raw materials:

cyclohexenone

Downstream raw materials:

3-chlorocyclohexanone