S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-benzyloxycarbonyl sulfoximide

Base Information

Chemical Name:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-benzyloxycarbonyl sulfoximide
CAS No.:1147096-54-5
Molecular Formula:C₂₈H₂₂Cl₂N₄O₅S
Molecular Weight:597.478
Hs Code.:

Synonyms:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-benzyloxycarbonyl sulfoximide

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Chemical Property of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-benzyloxycarbonyl sulfoximide

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Technology Process of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-benzyloxycarbonyl sulfoximide

There total 8 articles about S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-benzyloxycarbonyl sulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1147096-74-9
C₁₆H₁₄ClNO₄S

: 229343-30-0
2-amino-5-chloro-N-(5-chloro-pyridin-2-yl)-benzamide

: 1147096-54-5
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-benzyloxycarbonyl sulfoximide

Guidance literature:: In tetrahydrofuran; at 10 - 30 ℃; for 12h; Inert atmosphere;

Reference yield:

: 114129-35-0
methyl 4-(methylsulfinyl)benzoate

: 1147096-54-5
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-benzyloxycarbonyl sulfoximide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium azide; sulfuric acid / chloroform / 15 h / -20 - 50 °C / Inert atmosphere

2.1: pyridine / dichloromethane / 3 h / 15 - 30 °C / Inert atmosphere

3.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 25 - 30 °C

3.2: 0 °C

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

5.1: tetrahydrofuran / 12 h / 10 - 30 °C / Inert atmosphere

With pyridine; sodium azide; oxalyl dichloride; sulfuric acid; water; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; chloroform;

Reference yield:

: 3795-79-7
methyl 4-(methylthio)benzoate

: 1147096-54-5
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-benzyloxycarbonyl sulfoximide

Guidance literature:: Multi-step reaction with 6 steps

1.1: vanadia / acetonitrile / -25 - -20 °C / Inert atmosphere

1.2: 25 - 30 °C

2.1: sodium azide; sulfuric acid / chloroform / 15 h / -20 - 50 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 3 h / 15 - 30 °C / Inert atmosphere

4.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 25 - 30 °C

4.2: 0 °C

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

6.1: tetrahydrofuran / 12 h / 10 - 30 °C / Inert atmosphere

With pyridine; sodium azide; oxalyl dichloride; sulfuric acid; water; vanadia; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; chloroform; acetonitrile;