3,10-bis[(2-aminoethyl)amino]-6,13-dichloro[1,4]benzoxazino[2,3-b]phenoxazine-4,11-disulfonic acid

Base Information

• Chemical Name: 3,10-bis[(2-aminoethyl)amino]-6,13-dichloro[1,4]benzoxazino[2,3-b]phenoxazine-4,11-disulfonic acid
• CAS No.: 60316-87-2
• Molecular Formula: C₂₂H₂₀Cl₂N₆O₈S₂
• Molecular Weight: 631.474

Synonyms:3,10-bis(beta-aminoethylamino)-6,13-dichloro-4,11-disulphotriphenodioxazine

Chemical Property of 3,10-bis[(2-aminoethyl)amino]-6,13-dichloro[1,4]benzoxazino[2,3-b]phenoxazine-4,11-disulfonic acid

Chemical Property:

• PKA: -2.23±0.40(Predicted)
• Density: 1.95±0.1 g/cm3(Predicted)

Purity/Quality:

>=99.0% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 3,10-bis[(2-aminoethyl)amino]-6,13-dichloro[1,4]benzoxazino[2,3-b]phenoxazine-4,11-disulfonic acid

There total 1 articles about 3,10-bis[(2-aminoethyl)amino]-6,13-dichloro[1,4]benzoxazino[2,3-b]phenoxazine-4,11-disulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3,10-bis(beta-aminoethylamino)-6,13-dichloro-4,11-disulphotriphenodioxazine (60316-87-2)

Guidance literature:

Reference yield:

nicotinic acid (59-67-6) + 1,3,5-trichloro-2,4,6-triazine (108-77-0) + 3,10-bis(beta-aminoethylamino)-6,13-dichloro-4,11-disulphotriphenodioxazine (60316-87-2) + 3-aminobenzenesulfonic acid (121-47-1) + 4-amino-5-hydroxy-2,7-naphthalene-disulfonic acid, monosodium salt (5460-09-3) + 1,3-phenylenediamine-4-sulphonic acid sodium salt → C84H52Cl2N26O38S10(8-)*10Na(1+)

Guidance literature:

3-aminobenzenesulfonic acid; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃; for 1h;

4-amino-5-hydroxy-2,7-naphthalene-disulfonic acid, monosodium salt; With sodium hydrogencarbonate; In water; at 5 - 8 ℃; for 5h; pH=3 - 3.5;

nicotinic acid; 1,3,5-trichloro-2,4,6-triazine; 3,10-bis(beta-aminoethylamino)-6,13-dichloro-4,11-disulphotriphenodioxazine; 1,3-phenylenediamine-4-sulphonic acid sodium salt; Further stages;

Reference yield:

nicotinic acid (59-67-6) + 1,3,5-trichloro-2,4,6-triazine (108-77-0) + 3,10-bis(beta-aminoethylamino)-6,13-dichloro-4,11-disulphotriphenodioxazine (60316-87-2) + 4-amino-5-hydroxy-2,7-naphthalene-disulfonic acid, monosodium salt (5460-09-3) + 1,3-phenylenediamine-4-sulphonic acid sodium salt + 4-aminobenzene sulfonic acid (121-57-3,856062-06-1) → C84H52Cl2N26O38S10(8-)*10Na(1+)

Guidance literature:

4-aminobenzene sulfonic acid; With hydrogenchloride; sodium nitrite; In water; at 5 - 8 ℃; for 1h;

4-amino-5-hydroxy-2,7-naphthalene-disulfonic acid, monosodium salt; With sodium hydrogencarbonate; In water; at 5 - 8 ℃; for 5.5h; pH=3 - 3.5;

nicotinic acid; 1,3,5-trichloro-2,4,6-triazine; 3,10-bis(beta-aminoethylamino)-6,13-dichloro-4,11-disulphotriphenodioxazine; 1,3-phenylenediamine-4-sulphonic acid sodium salt; Further stages;

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