5-(4-guanidinophenyl)isoxazole-3-carboxylic acid methyl ester hydrochloride

Base Information

Chemical Name:5-(4-guanidinophenyl)isoxazole-3-carboxylic acid methyl ester hydrochloride
CAS No.:1612893-54-5
Molecular Formula:C₁₃H₁₄N₄O₃*ClH
Molecular Weight:310.74
Hs Code.:

Synonyms:5-(4-guanidinophenyl)isoxazole-3-carboxylic acid methyl ester hydrochloride

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Chemical Property of 5-(4-guanidinophenyl)isoxazole-3-carboxylic acid methyl ester hydrochloride

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Technology Process of 5-(4-guanidinophenyl)isoxazole-3-carboxylic acid methyl ester hydrochloride

There total 4 articles about 5-(4-guanidinophenyl)isoxazole-3-carboxylic acid methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 908802-68-6
ethyl 5-(4-amino-phenyl)isoxazole-3-carboxylate

: 420-04-2
CYANAMID

: 1612893-54-5
5-(4-guanidinophenyl)isoxazole-3-carboxylic acid methyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; water; for 8h; Reflux;

Reference yield:

: 54808-56-9
4-(4-nitrophenyl)-2,4-dione-butyric acid ethyl ester

: 1612893-54-5
5-(4-guanidinophenyl)isoxazole-3-carboxylic acid methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride / ethanol / 4 h / Reflux

2: tin(II) chloride dihdyrate / ethyl acetate / 6 h / Reflux

3: hydrogenchloride / ethanol; water / 8 h / Reflux

With hydrogenchloride; tin(II) chloride dihdyrate; hydroxylamine hydrochloride; In ethanol; water; ethyl acetate;
DOI:10.1016/j.bmcl.2014.04.118

Reference yield:

: 159670-70-9
ethyl 5-(4-nitrophenyl)isoxazole-3-carboxylate

: 1612893-54-5
5-(4-guanidinophenyl)isoxazole-3-carboxylic acid methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: tin(II) chloride dihdyrate / ethyl acetate / 6 h / Reflux

2: hydrogenchloride / ethanol; water / 8 h / Reflux

With hydrogenchloride; tin(II) chloride dihdyrate; In ethanol; water; ethyl acetate;
DOI:10.1016/j.bmcl.2014.04.118