Technology Process of C18H24O7
There total 2 articles about C18H24O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
ethyl 3-hydroxyphenylacetate;
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.333333h;
Inert atmosphere;
ethyl 3-bromo-2-(ethoxycarbonyl)propionate;
In
N,N-dimethyl-formamide;
at 110 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sulfuric acid / Reflux
2.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere
2.2: 110 °C / Inert atmosphere
With
sulfuric acid; sodium hydride;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: polyphosphoric acid / toluene / Reflux
2.1: sodium hydroxide; water / methanol / 2 h / 20 °C
2.2: pH 2
3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 1520.1 Torr
With
water; hydrogen; sodium hydroxide;
palladium 10% on activated carbon;
In
methanol; toluene;