3-Diphenylphosphinoylpropyl benzyl ether

Base Information

Chemical Name:3-Diphenylphosphinoylpropyl benzyl ether
CAS No.:246253-21-4
Molecular Formula:C₂₂H₂₃O₂P
Molecular Weight:350.397
Hs Code.:

Synonyms:3-Diphenylphosphinoylpropyl benzyl ether

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Chemical Property of 3-Diphenylphosphinoylpropyl benzyl ether

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Technology Process of 3-Diphenylphosphinoylpropyl benzyl ether

There total 1 articles about 3-Diphenylphosphinoylpropyl benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 889-57-6
3-(diphenylphosphinoyl)-1-propanol

: 100-39-0
benzyl bromide

: 246253-21-4
3-Diphenylphosphinoylpropyl benzyl ether

Guidance literature:: 3-(diphenylphosphinoyl)-1-propanol; With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;

benzyl bromide; In tetrahydrofuran; for 16h;
DOI:10.1039/a903370j

Reference yield: 82.0%

: 98-01-1
furfural

: 246253-21-4
3-Diphenylphosphinoylpropyl benzyl ether

: (1R*,2S*)-4-Benzyloxy-2-diphenylphosphinoyl-1-(2-furyl)butan-1-ol

: (1S*,1S*)-4-Benzyloxy-2-diphenylphosphinoyl-1-(2-furyl)butan-1-ol

Guidance literature:: 3-Diphenylphosphinoylpropyl benzyl ether; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;

furfural; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.5h;
DOI:10.1039/a903370j

Reference yield: 73.0%

: 123-11-5
4-methoxy-benzaldehyde

: 246253-21-4
3-Diphenylphosphinoylpropyl benzyl ether

: (1R*,2S*)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)butan-1-ol

: (1S*,2S*)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)butan-1-ol

Guidance literature:: 3-Diphenylphosphinoylpropyl benzyl ether; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;

4-methoxy-benzaldehyde; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.5h;
DOI:10.1039/a903370j