N'-[6-(3,5-dimethylpyrazol-1-yl)-s-tetrazin-3-yl]-4-methylfurazan-3-carbohydrazide

Base Information

• Chemical Name: N'-[6-(3,5-dimethylpyrazol-1-yl)-s-tetrazin-3-yl]-4-methylfurazan-3-carbohydrazide
• CAS No.: 1403740-29-3
• Molecular Formula: C₁₁H₁₂N₁₀O₂
• Molecular Weight: 316.282
• Mol file: 1403740-29-3.mol

Synonyms:N'-[6-(3,5-dimethylpyrazol-1-yl)-s-tetrazin-3-yl]-4-methylfurazan-3-carbohydrazide

Chemical Property of N'-[6-(3,5-dimethylpyrazol-1-yl)-s-tetrazin-3-yl]-4-methylfurazan-3-carbohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N'-[6-(3,5-dimethylpyrazol-1-yl)-s-tetrazin-3-yl]-4-methylfurazan-3-carbohydrazide

There total 4 articles about N'-[6-(3,5-dimethylpyrazol-1-yl)-s-tetrazin-3-yl]-4-methylfurazan-3-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3,6-bis-(3,5-dimethyl-pyrazol-1-yl)-1,2,4,5-tetrazine (30169-25-6) + 3-methylfurazancarboxylic hydrazide (32551-34-1) + isopropyl alcohol (67-63-0,8013-70-5) → 3,5-dimethyl-1H-pyrazole (67-51-6) + 3-(3,5-dimethylpyrazol-1-yl)-6-(iso-propoxy)-s-tetrazine (1403677-34-8) + N'-[6-(3,5-dimethylpyrazol-1-yl)-s-tetrazin-3-yl]-4-methylfurazan-3-carbohydrazide (1403740-29-3)

Guidance literature:

at 82 ℃; for 3h;

DOI:10.1007/s11172-012-0017-6

Reference yield: 78.0%

3,6-bis-(3,5-dimethyl-pyrazol-1-yl)-1,2,4,5-tetrazine (30169-25-6) + 3-methylfurazancarboxylic hydrazide (32551-34-1) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 3,5-dimethyl-1H-pyrazole (67-51-6) + N'-[6-(3,5-dimethylpyrazol-1-yl)-s-tetrazin-3-yl]-4-methylfurazan-3-carbohydrazide (1403740-29-3) + 3-(3,5-dimethylpyrazol-1-yl)-6-(N,N-dimethylamino)-s-tetrazine

Guidance literature:

at 90 ℃; for 4h;

DOI:10.1007/s11172-012-0017-6

Reference yield: 47.0%

3,6-bis-(3,5-dimethyl-pyrazol-1-yl)-1,2,4,5-tetrazine (30169-25-6) + ethanol (64-17-5) + 3-methylfurazancarboxylic hydrazide (32551-34-1) → 3,5-dimethyl-1H-pyrazole (67-51-6) + 3-(3,5-dimethyl-1H-pyrazol-1-yl)-6-ethoxy-1,2,4,5-tetrazine (1202249-08-8) + N'-[6-(3,5-dimethylpyrazol-1-yl)-s-tetrazin-3-yl]-4-methylfurazan-3-carbohydrazide (1403740-29-3)

Guidance literature:

at 78 ℃; for 2h;

DOI:10.1007/s11172-012-0017-6

upstream raw materials:

methanol

3,6-bis-(3,5-dimethyl-pyrazol-1-yl)-1,2,4,5-tetrazine

3-methylfurazancarboxylic hydrazide

ethanol