(E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-amine

Base Information

Chemical Name:(E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-amine
CAS No.:1353547-73-5
Molecular Formula:C₁₈H₂₂N₂O₆S
Molecular Weight:394.448
Hs Code.:

Synonyms:(E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-amine

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Chemical Property of (E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-amine

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Technology Process of (E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-amine

There total 8 articles about (E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1353547-72-4
(E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine

: 1353547-73-5
(E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-amine

Guidance literature:: (E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine; With iron; acetic acid; In methanol; at 50 ℃; for 2h; Inert atmosphere;

With ammonia; In water;

Reference yield:

: 23056-40-8
2-chloro-5-methyl-3-nitro-pyridine

: 1353547-73-5
(E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-amine

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium / 4 h / Reflux; Inert atmosphere

2.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 48 h / Inert atmosphere; Reflux

3.1: sodium carbonate / methanol / 1 h / 20 °C

4.1: dihydrogen peroxide; acetic acid / 6 h / 60 °C

5.1: water; sodium carbonate / methanol / 4 h / 20 °C

5.2: pH 2

6.1: piperidine; pyridine / 3 h / Inert atmosphere; Reflux

7.1: acetic acid; iron / methanol / 2 h / 50 °C / Inert atmosphere

With piperidine; pyridine; N-Bromosuccinimide; water; dihydrogen peroxide; sodium; iron; sodium carbonate; acetic acid; dibenzoyl peroxide; In methanol; tetrachloromethane;

Reference yield:

: 1353547-93-9
methyl 2-(((6-methoxy-5-nitropyridin-3-yl)methyl)sulfonyl)acetate

: 1353547-73-5
(E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium carbonate / methanol / 4 h / 20 °C

1.2: pH 2

2.1: piperidine; pyridine / 3 h / Inert atmosphere; Reflux

3.1: acetic acid; iron / methanol / 2 h / 50 °C / Inert atmosphere

With piperidine; pyridine; water; iron; sodium carbonate; acetic acid; In methanol;