(E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine

Base Information

Chemical Name:(E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine
CAS No.:1353547-72-4
Molecular Formula:C₁₈H₂₀N₂O₈S
Molecular Weight:424.431
Hs Code.:

Synonyms:(E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine

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Chemical Property of (E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine

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Technology Process of (E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine

There total 7 articles about (E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 830-79-5
2,4,6-trimethoxybenzaldehyde

: 1353547-94-0
2-(((6-methoxy-5-nitropyridin-3-yl)methyl)sulfonyl)acetic acid

: 1353547-72-4
(E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine

Guidance literature:: With piperidine; benzoic acid; In toluene; for 3h; Reflux; Inert atmosphere; Dean-Stark;
DOI:10.1021/jm4019614

Reference yield:

: 23056-40-8
2-chloro-5-methyl-3-nitro-pyridine

: 1353547-72-4
(E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium / 4 h / Reflux; Inert atmosphere

2.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 48 h / Inert atmosphere; Reflux

3.1: sodium carbonate / methanol / 1 h / 20 °C

4.1: dihydrogen peroxide; acetic acid / 6 h / 60 °C

5.1: water; sodium carbonate / methanol / 4 h / 20 °C

5.2: pH 2

6.1: piperidine; pyridine / 3 h / Inert atmosphere; Reflux

With piperidine; pyridine; N-Bromosuccinimide; water; dihydrogen peroxide; sodium; sodium carbonate; acetic acid; dibenzoyl peroxide; In methanol; tetrachloromethane;

Reference yield:

: 1353547-90-6
5-(bromomethyl)-2-methoxy-3-nitropyridine

: 1353547-72-4
(E)-2-methoxy-3-nitro-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / methanol / 1 h / 20 °C

2.1: dihydrogen peroxide; acetic acid / 6 h / 60 °C

3.1: water; sodium carbonate / methanol / 4 h / 20 °C

3.2: pH 2

4.1: piperidine; pyridine / 3 h / Inert atmosphere; Reflux

With piperidine; pyridine; water; dihydrogen peroxide; sodium carbonate; acetic acid; In methanol;