2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Base Information

Chemical Name:2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane
CAS No.:1394025-02-5
Molecular Formula:C₂₇H₂₉BO₃
Molecular Weight:412.336
Hs Code.:

Synonyms:2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

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Chemical Property of 2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Chemical Property:

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Technology Process of 2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

There total 4 articles about 2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 25354-48-7
1-bromo-1-(p-methoxyphenyl)-2,2-diphenylethene

: 73183-34-3
bis(pinacol)diborane

: 1394025-02-5
2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium phenolate; triphenylphosphine; In toluene; at 70 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.dyepig.2013.07.008

Reference yield:

: 18648-74-3
2,2-diphenyl-1-(4-methoxyphenyl)ethylene

: 1394025-02-5
2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / chloroform / 20 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; potassium phenolate; triphenylphosphine / toluene / 12 h / 70 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; potassium phenolate; bromine; triphenylphosphine; In chloroform; toluene;
DOI:10.1016/j.tet.2012.06.096

Reference yield:

: 19838-89-2
2-(4-methoxyphenyl)-1,1-diphenylethan-1-ol

: 1394025-02-5
2-[1-(4-methoxyphenyl)-2,2-diphenylvinyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / 0.08 h / Inert atmosphere; Reflux

2: bromine / chloroform / 20 °C / Inert atmosphere

3: bis-triphenylphosphine-palladium(II) chloride; potassium phenolate; triphenylphosphine / toluene / 12 h / 70 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; formic acid; potassium phenolate; bromine; triphenylphosphine; In chloroform; toluene;
DOI:10.1016/j.tet.2012.06.096