2-FLUORO-2'-NITRODIPHENYLAMINE

Base Information

• Chemical Name: 2-FLUORO-2'-NITRODIPHENYLAMINE
• CAS No.: 28898-02-4
• Molecular Formula: C12H9FN2O2
• Molecular Weight: 232.214
• Hs Code.: 2921420090
• Mol file: 28898-02-4.mol

Synonyms:Diphenylamine,2-fluoro-2'-nitro- (8CI);N-(2-Nitrophenyl)-2-fluoroaniline;NSC 93379;2-fluoro-N-(2-nitrophenyl)aniline;benzenamine, 2-fluoro-N-(2-nitrophenyl)-;

Chemical Property of 2-FLUORO-2'-NITRODIPHENYLAMINE

Chemical Property:

• Vapor Pressure: 0.000216mmHg at 25°C
• Refractive Index: 1.644
• Boiling Point: 326.4 °C at 760 mmHg
• Flash Point: 151.2 °C
• PSA: 57.85000
• Density: 1.353 g/cm³
• LogP: 4.07370

Purity/Quality:

97% ^*data from raw suppliers

2-Fluoro-2''-nitrodiphenylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-FLUORO-2'-NITRODIPHENYLAMINE

There total 5 articles about 2-FLUORO-2'-NITRODIPHENYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-Fluoro-2-iodobenzene (348-52-7) + 2-nitro-aniline (88-74-4) → N-(2-Fluorophenyl)-2-nitrobenzeneamine (28898-02-4)

Guidance literature:

With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; at 120 ℃; for 24h; Inert atmosphere; Sealed tube;

DOI:10.1021/jo302795w

Reference yield: 74.1%

2-Fluoroaniline (348-54-9) + ortho-nitrofluorobenzene (1493-27-2,127723-77-7) → N-(2-Fluorophenyl)-2-nitrobenzeneamine (28898-02-4)

Guidance literature:

2-Fluoroaniline; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

ortho-nitrofluorobenzene; In N,N-dimethyl-formamide; at 25 ℃; for 16h;

DOI:10.1016/j.bmc.2017.06.037

Reference yield: 72.0%

copper (12775-96-1,15158-11-9,15721-63-8,16941-75-6,17493-86-6,19498-52-3,20499-83-6,20499-84-7,20499-85-8,20499-86-9,20573-10-8,20573-11-9,21595-51-7,21595-52-8,22206-52-6,26445-28-3,28959-95-7,37362-93-9,39417-05-5,54603-16-6,54603-23-5,54603-32-6,54603-40-6,54603-48-4,54603-81-5,54603-89-3,56316-56-4,95985-91-4,122297-32-9,7440-50-8) + 2-nitro-aniline (88-74-4) + ortho-nitrofluorobenzene (1493-27-2,127723-77-7) → N-(2-Fluorophenyl)-2-nitrobenzeneamine (28898-02-4)

Guidance literature:

With potassium carbonate; In 5,5-dimethyl-1,3-cyclohexadiene; ethyl acetate;

upstream raw materials:

2-Fluoroaniline

ortho-nitrofluorobenzene

copper

2-nitro-aniline

Downstream raw materials:

N¹-(2-aminophenyl)-N¹-butyl-N²-(2-fluorophenyl)-N²-methylbenzene-1,2-diamine

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