4-(9-(2,4-dichlorophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8-octahydroacridin-10(9H)-yl)-N-(4-sulfamoylphenyl)benzamide

Base Information

• Chemical Name: 4-(9-(2,4-dichlorophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8-octahydroacridin-10(9H)-yl)-N-(4-sulfamoylphenyl)benzamide
• CAS No.: 1452583-40-2
• Molecular Formula: C₃₂H₂₇Cl₂N₃O₅S
• Molecular Weight: 636.555

Synonyms:4-(9-(2,4-dichlorophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8-octahydroacridin-10(9H)-yl)-N-(4-sulfamoylphenyl)benzamide

Chemical Property of 4-(9-(2,4-dichlorophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8-octahydroacridin-10(9H)-yl)-N-(4-sulfamoylphenyl)benzamide

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Technology Process of 4-(9-(2,4-dichlorophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8-octahydroacridin-10(9H)-yl)-N-(4-sulfamoylphenyl)benzamide

There total 4 articles about 4-(9-(2,4-dichlorophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8-octahydroacridin-10(9H)-yl)-N-(4-sulfamoylphenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

4-amino-N-(4-sulfamoylphenyl)benzamide (4389-05-3) + 1,3-cylohexanedione (504-02-9) + 2,4-dichlorobenzaldeyhde (874-42-0) → 4-(9-(2,4-dichlorophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8-octahydroacridin-10(9H)-yl)-N-(4-sulfamoylphenyl)benzamide (1452583-40-2)

Guidance literature:

With para-dodecylbenzenesulfonic acid; In water; for 24h; Reflux;

DOI:10.1016/j.bmc.2013.07.014

Reference yield:

4-nitro-benzoyl chloride (122-04-3) → 4-(9-(2,4-dichlorophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8-octahydroacridin-10(9H)-yl)-N-(4-sulfamoylphenyl)benzamide (1452583-40-2)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 5 h / 20 °C

2: sodiumsulfide nonahydrate; sulfur / ethanol; water

3: para-dodecylbenzenesulfonic acid / water / 24 h / Reflux

With sodiumsulfide nonahydrate; para-dodecylbenzenesulfonic acid; sulfur; triethylamine; In tetrahydrofuran; ethanol; water;

DOI:10.1016/j.bmc.2013.07.014

Reference yield:

sulfanilamide (63-74-1) → 4-(9-(2,4-dichlorophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8-octahydroacridin-10(9H)-yl)-N-(4-sulfamoylphenyl)benzamide (1452583-40-2)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 5 h / 20 °C

2: sodiumsulfide nonahydrate; sulfur / ethanol; water

3: para-dodecylbenzenesulfonic acid / water / 24 h / Reflux

With sodiumsulfide nonahydrate; para-dodecylbenzenesulfonic acid; sulfur; triethylamine; In tetrahydrofuran; ethanol; water;

DOI:10.1016/j.bmc.2013.07.014

upstream raw materials:

4-nitro-benzoyl chloride

sulfanilamide

N-(4-(aminosulfonyl)phenyl)-4-nitrobenzamide

4-amino-N-(4-sulfamoylphenyl)benzamide

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